Abstract

A compact and robust all-fiber difference frequency generation-based source of broadband mid-infrared radiation is presented. The source emits tunable radiation in the range between 6.5 µm and 9 µm with an average output power up to 5 mW at 125 MHz repetition frequency. The all-in-fiber construction of the source along with active stabilization techniques results in long-term repetition rate stability of 3 Hz per 10 h and a standard deviation of the output power better than 0.8% per 1 h. The applicability of the presented source to laser spectroscopy is demonstrated by measuring the absorption spectrum of nitrous oxide (N2O) around 7.8 µm. The robustness and good long- and short-term stability of the source opens up for applications outside the laboratory.

© 2019 Optical Society of America under the terms of the OSA Open Access Publishing Agreement

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2019 (3)

2018 (5)

L. Jin, V. Sonnenschein, M. Yamanaka, H. Tomita, T. Iguchi, A. Sato, K. Nozawa, K. Yoshida, S.-I. Ninomiya, and N. Nishizawa, “3.1–5.2 µm Coherent MIR Frequency Comb Based on Yb-Doped Fiber Laser,” IEEE J. Sel. Top. Quantum Electron. 24(3), 1–7 (2018).
[Crossref]

C. Gaida, M. Gebhardt, T. Heuermann, F. Stutzki, C. Jauregui, J. Antonio-Lopez, A. Schülzgen, R. Amezcua-Correa, A. Tünnermann, I. Pupeza, and J. Limpert, “Watt-scale super-octave mid-infrared intrapulse difference frequency generation,” Light: Sci. Appl. 7(1), 94 (2018).
[Crossref]

J. Sotor, T. Martynkien, P. G. Schunemann, P. Mergo, L. Rutkowski, and G. Soboń, “All-fiber mid-infrared source tunable from 6 to 9 µm based on difference frequency generation in OP-GaP crystal,” Opt. Express 26(9), 11756–11763 (2018).
[Crossref]

G. Soboń, T. Martynkien, D. Tomaszewska, K. Tarnowski, P. Mergo, and J. Sotor, “All-in-fiber amplification and compression of coherent frequency-shifted solitons tunable in the 1800–2000  nm range,” Photonics Res. 6(5), 368–372 (2018).
[Crossref]

G. Ycas, F. R. Giorgetta, E. Baumann, I. Coddington, D. Herman, S. A. Diddams, and N. R. Newbury, “High-coherence mid-infrared dual-comb spectroscopy spanning 2.6 to 5.2 µm,” Nat. Photonics 12(4), 202–208 (2018).
[Crossref]

2017 (5)

G. Soboń, T. Martynkien, P. Mergo, L. Rutkowski, and A. Foltynowicz, “High-power frequency comb source tunable from 2.7 to 4.2  µm based on difference frequency generation pumped by an Yb-doped fiber laser,” Opt. Lett. 42(9), 1748–1751 (2017).
[Crossref]

A. Krajewska, I. Pasternak, G. Sobon, J. Sotor, A. Przewloka, T. Ciuk, J. Sobieski, J. Grzonka, K. M. Abramski, and W. Strupinski, “Fabrication and applications of multi-layer graphene stack on transparent polymer,” Appl. Phys. Lett. 110(4), 041901 (2017).
[Crossref]

D. L. Maser, G. Ycas, W. I. Depetri, F. C. Cruz, and S. A. Diddams, “Coherent frequency combs for spectroscopy across the 3–5 µm region,” Appl. Phys. B 123(5), 142 (2017).
[Crossref]

J. C. Casals, S. Parsa, S. Chaitanya Kumar, K. Devi, P. G. Schunemann, and M. Ebrahim-Zadeh, “Picosecond difference-frequency-generation in orientation-patterned gallium phosphide,” Opt. Express 25(16), 19595–19602 (2017).
[Crossref]

I. E. Gordon, L. S. Rothman, C. Hill, R. V. Kochanov, Y. Tan, P. F. Bernath, M. Birk, V. Boudon, A. Campargue, K. V. Chance, B. J. Drouin, J.-M. Flaud, R. R. Gamache, J. T. Hodges, D. Jacquemart, V. I. Perevalov, A. Perrin, K. P. Shine, M.-A. H. Smith, P. J. Tennyson, G. C. Toon, H. Tran, V. G. Tyuterev, A. Barbe, A. G. Csaszar, V. M. Devi, T. Furtenbacher, J. J. Harrison, J.-M. Hartmannn, A. Jolly, T. J. Johnson, T. Karman, I. Kleiner, A. A. Kyuberis, J. Loos, O. M. Lyulin, S. T. Massie, S. N. Mikhailenko, N. Moazzen-Ahmadi, H. S. P. Müller, O. V. Naumenko, A. V. Nikitin, O. L. Polyansky, M. Rey, M. Rotger, S. W. Sharpe, K. Sung, E. Starikova, S. A. Tashkun, J. Vander Auwera, G. Wagner, J. Wilzewski, P. Wcislo, S. Yu, and E. J. Zak, “The HITRAN2016 molecular spectroscopic database,” J. Quant. Spectrosc. Radiat. Transfer 203, 3–69 (2017).
[Crossref]

2016 (5)

2015 (3)

A. G. Griffith, R. K. W. Lau, J. Cardenas, Y. Okawachi, A. Mohanty, R. Fain, Y. H. D. Lee, M. Yu, C. T. Phare, C. B. Poitras, A. L. Gaeta, and M. Lipson, “Silicon-chip mid-infrared frequency comb generation,” Nat. Commun. 6(1), 6299 (2015).
[Crossref]

L. Tao, K. Sun, D. J. Miller, D. Pan, L. M. Golston, and M. A. Zondlo, “Low-power, open-path mobile sensing platform for high-resolution measurements of greenhouse gases and air pollutants,” Appl. Phys. B 119(1), 153–164 (2015).
[Crossref]

M. Beutler, I. Rimke, E. Büttner, P. Farinello, A. Agnesi, V. Badikov, D. Badikov, and V. Petrov, “Difference-frequency generation of ultrashort pulses in the mid-IR using Yb-fiber pump systems and AgGaSe2,” Opt. Express 23(3), 2730–2736 (2015).
[Crossref]

2014 (3)

2013 (2)

2012 (6)

C. R. Phillips, J. Jiang, C. Mohr, A. C. Lin, C. Langrock, M. Snure, D. Bliss, M. Zhu, I. Hartl, J. S. Harris, M. E. Fermann, and M. M. Fejer, “Widely tunable midinfrared difference frequency generation in orientation-patterned GaAs pumped with a femtosecond Tm-fiber system,” Opt. Lett. 37(14), 2928–2930 (2012).
[Crossref]

L. Nugent-Glandorf, T. Neely, F. Adler, A. J. Fleisher, K. C. Cossel, B. Bjork, T. Dinneen, J. Ye, and S. A. Diddams, “Mid-infrared virtually imaged phased array spectrometer for rapid and broadband trace gas detection,” Opt. Lett. 37(15), 3285–3287 (2012).
[Crossref]

N. Leindecker, A. Marandi, R. L. Byer, K. L. Vodopyanov, J. Jiang, I. Hartl, M. Fermann, and P. G. Schunemann, “Octave-spanning ultrafast OPO with 2.6-6.1 µm instantaneous bandwidth pumped by femtosecond Tm-fiber laser,” Opt. Express 20(7), 7046–7053 (2012).
[Crossref]

A. Schliesser, N. Picque, and T. W. Hänsch, “Mid-infrared frequency combs,” Nat. Photonics 6(7), 440–449 (2012).
[Crossref]

A. Ruehl, A. Gambetta, I. Hartl, M. E. Fermann, K. S. E. Eikema, and M. Marangoni, “Widely-tunable mid-infrared frequency comb source based on difference frequency generation,” Opt. Lett. 37(12), 2232–2234 (2012).
[Crossref]

K. Krzempek, R. Lewicki, L. Nähle, M. Fischer, J. Koeth, S. Belahsene, Y. Rouillard, L. Worschech, and F. K. Tittel, “Continuous wave, distributed feedback diode laser based sensor for trace-gas detection of ethane,” Appl. Phys. B 106(2), 251–255 (2012).
[Crossref]

2010 (1)

2009 (1)

2007 (1)

2006 (2)

U. Willer, M. Saraji, A. Khorsandi, P. Geiser, and W. Schade, “Near-and mid-infrared laser monitoring of industrial processes, environment and security applications,” Opt. Laser Eng. 44(7), 699–710 (2006).
[Crossref]

J. Takayanagi, T. Sugiura, M. Yoshida, and N. Nishizawa, “1.0-1.7-µm Wavelength-Tunable Ultrashort-Pulse Generation Using Femtosecond Yb-Doped Fiber Laser and Photonic Crystal Fiber,” IEEE Photonics Technol. Lett. 18(21), 2284–2286 (2006).
[Crossref]

2004 (2)

2000 (1)

S. N. Bagayev, S. V. Chepurov, V. M. Klementyev, S. A. Kuznetsov, V. S. Pivtsov, V. V. Pokasov, and V. F. Zakharyash, “A femtosecond self-mode-locked Ti: sapphire laser with high stability of pulse-repetition frequency and its applications,” Appl. Phys. B 70(3), 375–378 (2000).
[Crossref]

1978 (1)

R. H. Stolen and C. Lin, “Self-phase-modulation in silica optical fibers,” Phys. Rev. A 17(4), 1448–1453 (1978).
[Crossref]

Abramski, K. M.

A. Krajewska, I. Pasternak, G. Sobon, J. Sotor, A. Przewloka, T. Ciuk, J. Sobieski, J. Grzonka, K. M. Abramski, and W. Strupinski, “Fabrication and applications of multi-layer graphene stack on transparent polymer,” Appl. Phys. Lett. 110(4), 041901 (2017).
[Crossref]

K. Krzempek, G. Sobon, and K. M. Abramski, “DFG-based mid-IR generation using a compact dual-wavelength all-fiber amplifier for laser spectroscopy applications,” Opt. Express 21(17), 20023–20031 (2013).
[Crossref]

Adler, F.

Agnesi, A.

Amezcua-Correa, R.

C. Gaida, M. Gebhardt, T. Heuermann, F. Stutzki, C. Jauregui, J. Antonio-Lopez, A. Schülzgen, R. Amezcua-Correa, A. Tünnermann, I. Pupeza, and J. Limpert, “Watt-scale super-octave mid-infrared intrapulse difference frequency generation,” Light: Sci. Appl. 7(1), 94 (2018).
[Crossref]

Antonio-Lopez, J.

C. Gaida, M. Gebhardt, T. Heuermann, F. Stutzki, C. Jauregui, J. Antonio-Lopez, A. Schülzgen, R. Amezcua-Correa, A. Tünnermann, I. Pupeza, and J. Limpert, “Watt-scale super-octave mid-infrared intrapulse difference frequency generation,” Light: Sci. Appl. 7(1), 94 (2018).
[Crossref]

Badikov, D.

Badikov, V.

Bagayev, S. N.

S. N. Bagayev, S. V. Chepurov, V. M. Klementyev, S. A. Kuznetsov, V. S. Pivtsov, V. V. Pokasov, and V. F. Zakharyash, “A femtosecond self-mode-locked Ti: sapphire laser with high stability of pulse-repetition frequency and its applications,” Appl. Phys. B 70(3), 375–378 (2000).
[Crossref]

Barbe, A.

I. E. Gordon, L. S. Rothman, C. Hill, R. V. Kochanov, Y. Tan, P. F. Bernath, M. Birk, V. Boudon, A. Campargue, K. V. Chance, B. J. Drouin, J.-M. Flaud, R. R. Gamache, J. T. Hodges, D. Jacquemart, V. I. Perevalov, A. Perrin, K. P. Shine, M.-A. H. Smith, P. J. Tennyson, G. C. Toon, H. Tran, V. G. Tyuterev, A. Barbe, A. G. Csaszar, V. M. Devi, T. Furtenbacher, J. J. Harrison, J.-M. Hartmannn, A. Jolly, T. J. Johnson, T. Karman, I. Kleiner, A. A. Kyuberis, J. Loos, O. M. Lyulin, S. T. Massie, S. N. Mikhailenko, N. Moazzen-Ahmadi, H. S. P. Müller, O. V. Naumenko, A. V. Nikitin, O. L. Polyansky, M. Rey, M. Rotger, S. W. Sharpe, K. Sung, E. Starikova, S. A. Tashkun, J. Vander Auwera, G. Wagner, J. Wilzewski, P. Wcislo, S. Yu, and E. J. Zak, “The HITRAN2016 molecular spectroscopic database,” J. Quant. Spectrosc. Radiat. Transfer 203, 3–69 (2017).
[Crossref]

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Baumann, E.

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U. Willer, M. Saraji, A. Khorsandi, P. Geiser, and W. Schade, “Near-and mid-infrared laser monitoring of industrial processes, environment and security applications,” Opt. Laser Eng. 44(7), 699–710 (2006).
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Figures (9)

Fig. 1.
Fig. 1. Schematic of the fiber-based Mid-IR comb source. PD – piezo driver, PID – PID controller, Mix – RF mixer, LO – local oscillator, FC – fiber coupler, DCF – dispersion compensating fiber, EDFA/TDFA – erbium/thulium doped fiber amplifier, PMF – polarization maintaining single-mode fiber, ODL – fiberized optical delay line, PZT – piezo-ceramic fiber stretcher, LA – logarithmic amplifier, BPF – electronic band-pass filter, DET – mid-IR detector, PCF – photonic crystal fiber, WDM – wavelength division multiplexer, COLL – collimator, FL – focusing lens, OPGaP - 3-mm long orientation patterned gallium phosphide crystal, BS – beam splitter. Electrical connections are shown in gray. Signal processing blocks responsible for stabilization are highlighted in dashed boxes.
Fig. 2.
Fig. 2. (a) The mode-locked seed laser setup, (b) the optical spectrum in a linear scale (inset shows the autocorrelation trace of the generated pulse), (c) the RF spectrum of the fundamental frep beatnote (inset shows the RF spectrum from DC to 6 GHz).
Fig. 3.
Fig. 3. (a) The peak power and average power of pulses launched into the PCF as a function of pump power delivered to the EDFA; (b) the Raman-shift-related evolution of the optical spectrum measured at the output of the highly nonlinear PCF recorded as a function of pulse peak power.
Fig. 4.
Fig. 4. (a) Optical spectra of pulses taking part in the DFG process, Autocorrelation traces of the 1560 nm pulses - (b) and the 1960nm pulses – (c).
Fig. 5.
Fig. 5. The optical spectra of the Mid-IR pulses generated in the nonlinear DFG process plotted as a function of the OPGaP crystal poling period. The average output power of the generated radiation is plotted in yellow stars - right Y-axis.
Fig. 6.
Fig. 6. Results of the repetition frequency stabilization of the ML seed laser. (a) The RF spectrum of the fundamental beatnote registered for extreme values of resonator temperature and voltage applied to the PZT stretcher incorporated into the resonator. (b) The time dependent pulse repetition frequency with active temperature stabilization of the fiber resonator at 30°C (blue shaded) and with active stabilization to a LO (red shaded). (c) The frequency response of the in-house built fiber PZT stretcher for a RMS voltage of ∼3.5 V.
Fig. 7.
Fig. 7. Integrated RIN spectral density in the range between 1 kHz and 100 kHz measured for the generated idler (left axis) and average idler output power (right axis) plotted in function of pump and signal pulse overlap (delay). Voltage ramp on the PZT element is plotted in blue. The 3 dB area of the RIN signal is shaded and corresponds to a delay offset of 4 fs.
Fig. 8.
Fig. 8. 60 minute heatmaps calculated from the DFG output spectra gathered every 60 seconds, with (a) the active stabilization turned OFF, and (b) ON. Panel (c) shows the output power stability for both cases measured as a function of time.
Fig. 9.
Fig. 9. Absorption spectrum of 0.75% N2O in N2 at 760 Torr (upper panel, black curve). A fit based on HITRAN parameters is plotted in red, and the residuum is shown in the lower panel.

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